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Information card for entry 4071129
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Coordinates | 4071129.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | DSiT-dimer |
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Chemical name | 2,2',3,3',6,6',7,7',14,14',15,15'-Dodeca(isopropoxy)- 10,10'-bis(trimethylsilyl)-,9,9'-bi-9,10-disilatriptycyl' |
Formula | C78 H114 O12 Si6 |
Calculated formula | C78 H114 O12 Si6 |
Title of publication | Synthesis and Electronic Spectra of Disilatriptycene Oligomers: Evidence for Electronic Delocalization along the One-Dimensional Arrangement of Bridge-Head Disilanes |
Authors of publication | Sase, Shohei; Cho, Yoen-Seok; Kawachi, Atsushi; Wakamiya, Atsushi; Yamaguchi, Shigehiro; Tsuji, Hayato; Tamao, Kohei |
Journal of publication | Organometallics |
Year of publication | 2008 |
Journal volume | 27 |
Journal issue | 21 |
Pages of publication | 5441 |
a | 18.2723 ± 0.0002 Å |
b | 11.9096 ± 0.0002 Å |
c | 18.6349 ± 0.0003 Å |
α | 90° |
β | 90.3209 ± 0.0009° |
γ | 90° |
Cell volume | 4055.18 ± 0.1 Å3 |
Cell temperature | 103 ± 2 K |
Ambient diffraction temperature | 103 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0591 |
Residual factor for significantly intense reflections | 0.0466 |
Weighted residual factors for significantly intense reflections | 0.1174 |
Weighted residual factors for all reflections included in the refinement | 0.1268 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.029 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4071129.html
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