Information card for entry 4071192

Structure parameters

• Formula: C42 H55 N2 Ni O P
• Calculated formula: C42 H48 N2 Ni O P
• Title of publication: Influence of Steric and Electronic Perturbations on the Polymerization Activities of α-Iminocarboxamide Nickel Complexes
• Authors of publication: Azoulay, Jason D.; Itigaki, Koji; Wu, Guang; Bazan, Guillermo C.
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 10
• Pages of publication: 2273
• a: 9.9429 ± 0.0007 Å
• b: 25.4501 ± 0.0019 Å
• c: 15.2227 ± 0.0011 Å
• α: 90°
• β: 93.662 ± 0.002°
• γ: 90°
• Cell volume: 3844.2 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1315
• Residual factor for significantly intense reflections: 0.0682
• Weighted residual factors for significantly intense reflections: 0.1465
• Weighted residual factors for all reflections included in the refinement: 0.1573
• Goodness-of-fit parameter for all reflections included in the refinement: 1.451
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No