Information card for entry 4071228

Structure parameters

• Formula: C17 H43 Cl Ir P3 Si
• Calculated formula: C17 H43 Cl Ir P3 Si
• Title of publication: Silapentadienyl−Iridium−Phosphine Chemistry(1)
• Authors of publication: Bleeke, John R.; Thananatthanachon, Todsapon; Rath, Nigam P.
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 11
• Pages of publication: 2436
• a: 9.3062 ± 0.0006 Å
• b: 10.7212 ± 0.0007 Å
• c: 12.1508 ± 0.0007 Å
• α: 90°
• β: 94.122 ± 0.003°
• γ: 90°
• Cell volume: 1209.19 ± 0.13 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0317
• Residual factor for significantly intense reflections: 0.0261
• Weighted residual factors for significantly intense reflections: 0.0446
• Weighted residual factors for all reflections included in the refinement: 0.046
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No