Information card for entry 4071293

Structure parameters

• Formula: C22 H54 Fe P4
• Calculated formula: C22 H54 Fe P4
• Title of publication: Addition of CO2to Alkyl Iron Complexes, Fe(PP)2Me2
• Authors of publication: Allen, Olivia R.; Dalgarno, Scott J.; Field, Leslie D.; Jensen, Paul; Turnbull, Anthony J.; Willis, Anthony C.
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 9
• Pages of publication: 2092
• a: 7.593 ± 0.0004 Å
• b: 10.2012 ± 0.0004 Å
• c: 19.5659 ± 0.001 Å
• α: 77.903 ± 0.002°
• β: 89.807 ± 0.002°
• γ: 68.634 ± 0.004°
• Cell volume: 1375.59 ± 0.12 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0686
• Residual factor for significantly intense reflections: 0.0565
• Weighted residual factors for significantly intense reflections: 0.1025
• Weighted residual factors for all reflections included in the refinement: 0.1069
• Goodness-of-fit parameter for all reflections included in the refinement: 1.123
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No