Information card for entry 4071316

Structure parameters

• Formula: C36 H86 N6 P2 Pb2 Si6
• Calculated formula: C36 H86 N6 P2 Pb2 Si6
• SMILES: [Pb]1([n]2ccnc(c2C=P(N1[Si](C)(C)C)(C(C)C)C(C)C)C1[Pb]([N]([Si](C)(C)C)=P1(C(C)C)C(C)C)N([Si](C)(C)C)[Si](C)(C)C)N([Si](C)(C)C)[Si](C)(C)C
• Title of publication: Synthesis of Heteroleptic Tin(II) and Lead(II) Compounds from Pyrazyl-Linked Bisphosphoranoimine
• Authors of publication: Leung, Wing-Por; Chan, Ka-Po; Kan, Kwok-Wai; Mak, Thomas C. W.
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 12
• Pages of publication: 2767
• a: 12.4223 ± 0.0015 Å
• b: 15.818 ± 0.002 Å
• c: 16.737 ± 0.002 Å
• α: 66.813 ± 0.002°
• β: 75.262 ± 0.002°
• γ: 69.288 ± 0.002°
• Cell volume: 2802.2 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0703
• Residual factor for significantly intense reflections: 0.0446
• Weighted residual factors for significantly intense reflections: 0.1146
• Weighted residual factors for all reflections included in the refinement: 0.1309
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No