Information card for entry 4071330

Structure parameters

• Formula: C23 H36 I3 N8 Rh
• Calculated formula: C23 H36 I3 N8 Rh
• Title of publication: Rhodium(III) Complexes Containing C4-Bound N-Heterocyclic Carbenes: Synthesis, Coordination Chemistry, and Catalytic Activity in Transfer Hydrogenation
• Authors of publication: Yang, Liangru; Krüger, Anneke; Neels, Antonia; Albrecht, Martin
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 13
• Pages of publication: 3161
• a: 22.766 ± 0.0009 Å
• b: 17.1487 ± 0.001 Å
• c: 18.2406 ± 0.0007 Å
• α: 90°
• β: 114.912 ± 0.003°
• γ: 90°
• Cell volume: 6458.7 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0448
• Residual factor for significantly intense reflections: 0.0303
• Weighted residual factors for significantly intense reflections: 0.07
• Weighted residual factors for all reflections included in the refinement: 0.0732
• Goodness-of-fit parameter for all reflections included in the refinement: 0.945
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No