Information card for entry 4071333

Structure parameters

• Formula: C148.5 H171 Cl16.5 N12 O1.5 P3 Rh3
• Calculated formula: C148.5 H171 Cl16.5 N12 O1.5 P3 Rh3
• Title of publication: Rhodium(III) Complexes Containing C4-Bound N-Heterocyclic Carbenes: Synthesis, Coordination Chemistry, and Catalytic Activity in Transfer Hydrogenation
• Authors of publication: Yang, Liangru; Krüger, Anneke; Neels, Antonia; Albrecht, Martin
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 13
• Pages of publication: 3161
• a: 15.964 ± 0.002 Å
• b: 19.617 ± 0.003 Å
• c: 25.72 ± 0.004 Å
• α: 94.133 ± 0.012°
• β: 101.237 ± 0.01°
• γ: 103.493 ± 0.01°
• Cell volume: 7624 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2865
• Residual factor for significantly intense reflections: 0.1008
• Weighted residual factors for significantly intense reflections: 0.2116
• Weighted residual factors for all reflections included in the refinement: 0.279
• Goodness-of-fit parameter for all reflections included in the refinement: 0.821
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No