Information card for entry 4071363

Structure parameters

• Formula: C32 H60 O17 P3 Re Sn
• Calculated formula: C32 H60 O17 P3 Re Sn
• SMILES: [Re](C#[O])(C#[O])([Sn](C(=C)C(=O)OC)(C(=C)C(=O)OC)C(=C)C(=O)OC)([P](OCC)(OCC)OCC)([P](OCC)(OCC)OCC)[P](OCC)(OCC)OCC
• Title of publication: Preparation of Trivinylstannyl Complexes of Manganese and Rhenium
• Authors of publication: Albertin, Gabriele; Antoniutti, Stefano; Castro, Jesús; Fontán, Soledad García; Zanardo, Gianluigi
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 12
• Pages of publication: 2789
• a: 10.7012 ± 0.0013 Å
• b: 22.898 ± 0.003 Å
• c: 20.818 ± 0.003 Å
• α: 90°
• β: 93.557 ± 0.003°
• γ: 90°
• Cell volume: 5091.3 ± 1.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0681
• Residual factor for significantly intense reflections: 0.0366
• Weighted residual factors for significantly intense reflections: 0.0834
• Weighted residual factors for all reflections included in the refinement: 0.0937
• Goodness-of-fit parameter for all reflections included in the refinement: 0.95
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No