Information card for entry 4071444

Structure parameters

• Formula: C45 H51 Cu N2 Sn
• Calculated formula: C45 H51 Cu N2 Sn
• Title of publication: Carbon−Carbon Bond Formation on Reaction of a Copper(I) Stannyl Complex with Carbon Dioxide
• Authors of publication: Bhattacharyya, Koyel X.; Akana, Jennifer A.; Laitar, David S.; Berlin, Jacob M.; Sadighi, Joseph P.
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 12
• Pages of publication: 2682
• a: 11.2582 ± 0.0005 Å
• b: 19.0392 ± 0.0008 Å
• c: 20.541 ± 0.0009 Å
• α: 86.344 ± 0.001°
• β: 76.811 ± 0.001°
• γ: 73.357 ± 0.001°
• Cell volume: 4107.2 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0384
• Residual factor for significantly intense reflections: 0.0308
• Weighted residual factors for significantly intense reflections: 0.0725
• Weighted residual factors for all reflections included in the refinement: 0.0768
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No