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Information card for entry 4071504
Preview
Coordinates | 4071504.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C54 H56 B Cl2 F10 N2 O3 P3 Ru |
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Calculated formula | C50 H48 B1.14 F6.82 N2 O5.328 P3.1887 Ru |
Title of publication | Acidic Ruthenium PNNP Complexes of Non-enolized 1,3-Dicarbonyl Compounds as Catalysts for Asymmetric Michael Addition |
Authors of publication | Santoro, Francesco; Althaus, Martin; Bonaccorsi, Cristina; Gischig, Sebastian; Mezzetti, Antonio |
Journal of publication | Organometallics |
Year of publication | 2008 |
Journal volume | 27 |
Journal issue | 15 |
Pages of publication | 3866 |
a | 12.046 ± 0.0005 Å |
b | 20.6031 ± 0.0009 Å |
c | 20.3481 ± 0.0009 Å |
α | 90° |
β | 92.702 ± 0.001° |
γ | 90° |
Cell volume | 5044.5 ± 0.4 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 9 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0631 |
Residual factor for significantly intense reflections | 0.0545 |
Weighted residual factors for significantly intense reflections | 0.1548 |
Weighted residual factors for all reflections included in the refinement | 0.1606 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.115 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4071504.html
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