Information card for entry 4071534

Structure parameters

• Common name: SiOSPt
• Formula: C78 H114 O P2 Pt S Si7
• Calculated formula: C78 H114 O P2 Pt S Si7
• Title of publication: Syntheses and Structures of Platinum Siloxides Bridged by a Sulfur or Selenium Atom and a Unique 1,3-Aryl Migration from Silicon to Platinum through the Si−O−Pt Linkages
• Authors of publication: Tanabe, Taro; Mizuhata, Yoshiyuki; Takeda, Nobuhiro; Tokitoh, Norihiro
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 10
• Pages of publication: 2156
• a: 13.5758 ± 0.0002 Å
• b: 16.686 ± 0.0004 Å
• c: 21.1691 ± 0.0004 Å
• α: 112.593 ± 0.0008°
• β: 102.713 ± 0.0007°
• γ: 91.7477 ± 0.0009°
• Cell volume: 4283.44 ± 0.15 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0444
• Residual factor for significantly intense reflections: 0.034
• Weighted residual factors for significantly intense reflections: 0.0781
• Weighted residual factors for all reflections included in the refinement: 0.0834
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No