Information card for entry 4071613

Structure parameters

• Formula: C30 H41 F3 Ge N2 O3 S
• Calculated formula: C30 H41 F3 Ge N2 O3 S
• Title of publication: Facile Access to a Stable Divalent Germanium Compound with a Terminal PH2Group and Related PR2Derivatives
• Authors of publication: Yao, Shenglai; Brym, Markus; Merz, Klaus; Driess, Matthias
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 14
• Pages of publication: 3601
• a: 12.087 ± 0.002 Å
• b: 13.013 ± 0.003 Å
• c: 24.046 ± 0.005 Å
• α: 90°
• β: 92.11 ± 0.03°
• γ: 90°
• Cell volume: 3779.6 ± 1.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1054
• Residual factor for significantly intense reflections: 0.0591
• Weighted residual factors for significantly intense reflections: 0.1381
• Weighted residual factors for all reflections included in the refinement: 0.1561
• Goodness-of-fit parameter for all reflections included in the refinement: 0.93
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No