Information card for entry 4071617

Structure parameters

• Formula: C36 H48 Ag4 Cl4 N12
• Calculated formula: C36 H48 Ag4 Cl4 N12
• Title of publication: Dinuclear Palladacyclic Complexes Derived from C−N Cleavage of an Imidazolium Salt: Synthesis, Structural Characterization, and Their Uses for C−C Coupling
• Authors of publication: Ye, Jiansheng; Zhang, Xiaoming; Chen, Wanzhi; Shimada, Shigeru
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 16
• Pages of publication: 4166
• a: 21.623 ± 0.003 Å
• b: 6.6427 ± 0.0015 Å
• c: 15.8766 ± 0.0019 Å
• α: 90°
• β: 100.017 ± 0.002°
• γ: 90°
• Cell volume: 2245.7 ± 0.7 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2361
• Residual factor for significantly intense reflections: 0.164
• Weighted residual factors for significantly intense reflections: 0.4135
• Weighted residual factors for all reflections included in the refinement: 0.4487
• Goodness-of-fit parameter for all reflections included in the refinement: 1.248
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No