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Information card for entry 4071654
Preview
Coordinates | 4071654.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C36 H51 Cl2 N3 P2 Ru |
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Calculated formula | C36 H51 Cl2 N3 P2 Ru |
SMILES | [Ru]12(Cl)(Cl)([P](Cc3[n]2c(ccc3)C[P]1(C(C)(C)C)C(C)(C)C)(C(C)(C)C)C(C)(C)C)[N]#N=C1c2ccccc2c2ccccc12 |
Title of publication | Stable Carbene and Diazoalkane Complexes of the Same Complex System. Synthesis, Structure, and Reactivity of PNP−Ru(II) Fluorenylidene and Diazofluorene Complexes |
Authors of publication | Zhang, Jing; Gandelman, Mark; Shimon, Linda J. W.; Milstein, David |
Journal of publication | Organometallics |
Year of publication | 2008 |
Journal volume | 27 |
Journal issue | 14 |
Pages of publication | 3526 |
a | 18.0783 ± 0.0003 Å |
b | 14.7973 ± 0.0003 Å |
c | 27.1111 ± 0.0006 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 7252.5 ± 0.2 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 6 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0786 |
Residual factor for significantly intense reflections | 0.0462 |
Weighted residual factors for significantly intense reflections | 0.1102 |
Weighted residual factors for all reflections included in the refinement | 0.1227 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.049 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4071654.html
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