Information card for entry 4071656

Structure parameters

• Formula: C39.25 H51 N3 O0.5 P2 Ru
• Calculated formula: C39.25 H51 N3 O0.5 P2 Ru
• Title of publication: Stable Carbene and Diazoalkane Complexes of the Same Complex System. Synthesis, Structure, and Reactivity of PNP−Ru(II) Fluorenylidene and Diazofluorene Complexes
• Authors of publication: Zhang, Jing; Gandelman, Mark; Shimon, Linda J. W.; Milstein, David
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 14
• Pages of publication: 3526
• a: 34.707 ± 0.007 Å
• b: 14.668 ± 0.003 Å
• c: 17.259 ± 0.004 Å
• α: 90°
• β: 117.57 ± 0.04°
• γ: 90°
• Cell volume: 7789 ± 4 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0692
• Residual factor for significantly intense reflections: 0.0537
• Weighted residual factors for significantly intense reflections: 0.1592
• Weighted residual factors for all reflections included in the refinement: 0.1707
• Goodness-of-fit parameter for all reflections included in the refinement: 1.095
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No