Information card for entry 4071683

Structure parameters

• Formula: C19 H19 N2 Rh
• Calculated formula: C19 H19 N2 Rh
• SMILES: [Rh]1234([n]5cccc6c=c7cccn1c7=c56)[CH]1=[CH]2CC[CH]3=[CH]4CC1
• Title of publication: Syntheses, Characterizations, and Reactivities of 4,5-Diazafluorenide Complexes of Palladium(II) and Rhodium(I)
• Authors of publication: Jiang, Huiling; Song, Datong
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 14
• Pages of publication: 3587
• a: 10.0544 ± 0.0004 Å
• b: 11.1105 ± 0.0005 Å
• c: 12.8356 ± 0.0003 Å
• α: 90°
• β: 97.249 ± 0.002°
• γ: 90°
• Cell volume: 1422.4 ± 0.09 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0345
• Residual factor for significantly intense reflections: 0.0272
• Weighted residual factors for significantly intense reflections: 0.0646
• Weighted residual factors for all reflections included in the refinement: 0.0686
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No