Information card for entry 4071719

Structure parameters

• Formula: C19 H29 N2 V
• Calculated formula: C19 H29 N2 V
• SMILES: [V]1234(=Nc5ccc(cc5)C)(N(C(C)C)C(C)C)([cH]5[cH]4[cH]3[cH]2[cH]15)C
• Title of publication: Relative Reactivity of the Metal−Amido versus Metal−Imido Bond in Linked Cp-Amido and Half-Sandwich Complexes of Vanadium
• Authors of publication: Bouwkamp, Marco W.; Batinas, Aurora A.; Witte, Peter T.; Hubregtse, Ton; Dam, Jeroen; Meetsma, Auke; Teuben, Jan H.; Hessen, Bart
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 16
• Pages of publication: 4071
• a: 13.38 ± 0.001 Å
• b: 11.0573 ± 0.0009 Å
• c: 13.949 ± 0.001 Å
• α: 90°
• β: 116.596 ± 0.001°
• γ: 90°
• Cell volume: 1845.3 ± 0.2 ų
• Cell temperature: 100 ± 1 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0831
• Residual factor for significantly intense reflections: 0.0525
• Weighted residual factors for significantly intense reflections: 0.1168
• Weighted residual factors for all reflections included in the refinement: 0.1292
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No