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Information card for entry 4071779
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Coordinates | 4071779.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C21 H20 O4 |
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Calculated formula | C21 H20 O4 |
Title of publication | Cascade Reactions of Dialkynyl Fischer Carbene Complexes Involving Intramolecular Alkyne Insertions Oriented to the Synthesis of Functionalized Polycycles |
Authors of publication | Barluenga, José; Fañanás-Mastral, Martín; Andina, Facundo; Aznar, Fernando; Valdés, Carlos |
Journal of publication | Organometallics |
Year of publication | 2008 |
Journal volume | 27 |
Journal issue | 14 |
Pages of publication | 3593 |
a | 8.0964 ± 0.0013 Å |
b | 8.8792 ± 0.0014 Å |
c | 12.731 ± 0.002 Å |
α | 86.206 ± 0.003° |
β | 75.741 ± 0.003° |
γ | 71.116 ± 0.003° |
Cell volume | 839.2 ± 0.2 Å3 |
Cell temperature | 298 ± 2 K |
Ambient diffraction temperature | 298 ± 2 K |
Number of distinct elements | 3 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0546 |
Residual factor for significantly intense reflections | 0.0441 |
Weighted residual factors for significantly intense reflections | 0.1151 |
Weighted residual factors for all reflections included in the refinement | 0.1236 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.044 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4071779.html
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Users of the data should acknowledge the original authors of the
structural data.