Information card for entry 4071791

Structure parameters

• Formula: C30 H50 Os3
• Calculated formula: C30 H45 Os3
• SMILES: [Os]12345([Os]6789([Os]%10%11%12%131[c]1([c]%13([c]%12([c]%11([c]%101C)C)C)C)C)[c]1([c]6([c]7([c]8([c]91C)C)C)C)C)[c]1([c]5([c]4([c]3([c]21C)C)C)C)C
• Title of publication: Synthesis of Trinuclear Osmium Polyhydrido Clusters [{(C5Me5)Os}3(μ-H)6]+and {(C5Me5)Os}3(μ-H)3(μ3-H)2and Comparison with the Ruthenium Analogues
• Authors of publication: Kameo, Hajime; Suzuki, Hiroharu
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 16
• Pages of publication: 4248
• a: 11.0085 ± 0.001 Å
• b: 11.0311 ± 0.0006 Å
• c: 15.1064 ± 0.0007 Å
• α: 71.327 ± 0.002°
• β: 73.298 ± 0.004°
• γ: 60.641 ± 0.004°
• Cell volume: 1495.67 ± 0.18 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0429
• Residual factor for significantly intense reflections: 0.0398
• Weighted residual factors for significantly intense reflections: 0.0968
• Weighted residual factors for all reflections included in the refinement: 0.0997
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No