Information card for entry 4071865

Structure parameters

• Formula: C54 H56 Ge4 P2 Pd
• Calculated formula: C54 H56 Ge4 P2 Pd
• SMILES: [Pd]12([Ge]([Ge]([Ge]([Ge]1(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)[P](C)(C)CC[P]2(C)C
• Title of publication: Mono- and Dinuclear Germapalladacycles Obtained via the Ge−Ge Bond Forming Reactions Promoted by Palladium Complexes
• Authors of publication: Tanabe, Makoto; Ishikawa, Naoko; Hanzawa, Masaya; Osakada, Kohtaro
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 19
• Pages of publication: 5152
• a: 22.863 ± 0.004 Å
• b: 21.865 ± 0.003 Å
• c: 30.131 ± 0.005 Å
• α: 90°
• β: 101.893 ± 0.002°
• γ: 90°
• Cell volume: 14739 ± 4 ų
• Cell temperature: 113.1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for significantly intense reflections: 0.0562
• Weighted residual factors for all reflections included in the refinement: 0.132
• Goodness-of-fit parameter for all reflections included in the refinement: 0.957
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No