Information card for entry 4071900

Structure parameters

• Formula: C34 H36 Cl6 N O2 Os P
• Calculated formula: C34 H32 Cl6 N O2 Os P
• Title of publication: Osmium-Catalyzed Allylic Alkylation
• Authors of publication: Esteruelas, Miguel A.; García-Yebra, Cristina; Oliván, Montserrat; Oñate, Enrique; Valencia, Marta
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 19
• Pages of publication: 4892
• a: 11.3914 ± 0.0017 Å
• b: 12.7982 ± 0.0019 Å
• c: 13.092 ± 0.0019 Å
• α: 90.109 ± 0.003°
• β: 107.61 ± 0.002°
• γ: 103.228 ± 0.003°
• Cell volume: 1765.7 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 1
• Hermann-Mauguin space group symbol: P 1
• Hall space group symbol: P 1
• Residual factor for all reflections: 0.0533
• Residual factor for significantly intense reflections: 0.0459
• Weighted residual factors for significantly intense reflections: 0.1091
• Weighted residual factors for all reflections included in the refinement: 0.1131
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No