Information card for entry 4071960

Structure parameters

• Formula: C146 H184 Ag8 F24 N24 O2 P4
• Calculated formula: C146 H184 Ag8 F24 N24 O2 P4
• Title of publication: Combining Pyrazolate and N-Heterocyclic Carbene Coordination Motifs: Synthesis and Characterization of a Double-Crowned Silver Complex
• Authors of publication: Scheele, Ulrich J.; Georgiou, Maria; John, Michael; Dechert, Sebastian; Meyer, Franc
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 19
• Pages of publication: 5146
• a: 19.2514 ± 0.0004 Å
• b: 21.4494 ± 0.0005 Å
• c: 23.7189 ± 0.0005 Å
• α: 80.184 ± 0.002°
• β: 82.059 ± 0.002°
• γ: 77.33 ± 0.002°
• Cell volume: 9364 ± 0.4 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0706
• Residual factor for significantly intense reflections: 0.0562
• Weighted residual factors for significantly intense reflections: 0.1506
• Weighted residual factors for all reflections included in the refinement: 0.1564
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No