Information card for entry 4071964

Structure parameters

• Formula: C76 H76 Cl4 F12 N4 O20 Rh4 S4
• Calculated formula: C73 H76 Cl4 F3 N4 O11 Rh4 S
• Title of publication: Stepwise Formation of Molecular Rectangles of Half-Sandwich Rhodium and Ruthenium Complexes Containing Bridging Chloranilate Ligands
• Authors of publication: Han, Ying-Feng; Jia, Wei-Guo; Lin, Yue-Jian; Jin, Guo-Xin
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 19
• Pages of publication: 5002
• a: 16.385 ± 0.009 Å
• b: 18.966 ± 0.01 Å
• c: 16.274 ± 0.009 Å
• α: 90°
• β: 92.407 ± 0.007°
• γ: 90°
• Cell volume: 5053 ± 5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1617
• Residual factor for significantly intense reflections: 0.0964
• Weighted residual factors for significantly intense reflections: 0.246
• Weighted residual factors for all reflections included in the refinement: 0.2867
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No