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Information card for entry 4072006
Preview
Coordinates | 4072006.cif |
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Original paper (by DOI) | HTML |
Formula | C33 H54 O P2 Ru |
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Calculated formula | C33 H54 O P2 Ru |
SMILES | C(#[O])[Ru]123([CH]#[CH]1)([CH]1CC(C[CH]2=1)[P]3(C1CCCC1)C1CCCC1)[P](C1CCCC1)(C1CCCC1)C1CCCC1 |
Title of publication | Access to Ruthenium(0) Carbonyl Complexes via Dehydrogenation of a Tricyclopentylphosphine Ligand and Decarbonylation of Alcohols |
Authors of publication | Bolton, Paul D.; Grellier, Mary; Vautravers, Nicolas; Vendier, Laure; Sabo-Etienne, Sylviane |
Journal of publication | Organometallics |
Year of publication | 2008 |
Journal volume | 27 |
Journal issue | 19 |
Pages of publication | 5088 |
a | 13.0141 ± 0.0006 Å |
b | 15.4869 ± 0.0008 Å |
c | 16.3101 ± 0.0007 Å |
α | 90° |
β | 110.853 ± 0.004° |
γ | 90° |
Cell volume | 3071.9 ± 0.3 Å3 |
Cell temperature | 110 K |
Ambient diffraction temperature | 110 K |
Number of distinct elements | 5 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0406 |
Residual factor for significantly intense reflections | 0.0353 |
Weighted residual factors for significantly intense reflections | 0.09 |
Weighted residual factors for all reflections included in the refinement | 0.0981 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.039 |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4072006.html
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