Information card for entry 4072036

Structure parameters

• Formula: C47.33 H69.66 B2 Cl0.66 F8 N3 Os P2
• Calculated formula: C47.33 H69.66 B2 Cl0.66 F8 N3 Os P2
• Title of publication: Formation of an Asymmetric Acyclic Osmium−Dienylcarbene Complex
• Authors of publication: Bolaño, Tamara; Castarlenas, Ricardo; Esteruelas, Miguel A.; Oñate, Enrique
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 23
• Pages of publication: 6367
• a: 21.522 ± 0.004 Å
• b: 14.461 ± 0.003 Å
• c: 19.434 ± 0.004 Å
• α: 90°
• β: 116.31 ± 0.003°
• γ: 90°
• Cell volume: 5421.9 ± 1.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1607
• Residual factor for significantly intense reflections: 0.0637
• Weighted residual factors for significantly intense reflections: 0.1343
• Weighted residual factors for all reflections included in the refinement: 0.1613
• Goodness-of-fit parameter for all reflections included in the refinement: 0.862
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No