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Information card for entry 4072073
Preview
Coordinates | 4072073.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22 H42 Cl O2 P Pd |
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Calculated formula | C22 H42 Cl O2 P Pd |
SMILES | [Pd]([C@@H]1[C@@H]([C@H]2[C@H](C[C@@H]1C2)C(=O)OC)C)(Cl)[P](C(C)(C)C)(C(C)(C)C)C(C)(C)C.[Pd]([C@H]1[C@H]([C@@H]2[C@@H](C[C@H]1C2)C(=O)OC)C)(Cl)[P](C(C)(C)C)(C(C)(C)C)C(C)(C)C |
Title of publication | Syntheses of Ester-Substituted Norbornyl Palladium Complexes Ligated withtBu3P: Studies on the Insertion ofexo- andendo-Monomers in the Ester-Substituted Norbornene Polymerization |
Authors of publication | Takamiya, Ikuko; Yamashita, Makoto; Nozaki, Kyoko |
Journal of publication | Organometallics |
Year of publication | 2008 |
Journal volume | 27 |
Journal issue | 20 |
Pages of publication | 5347 |
a | 8.592 ± 0.005 Å |
b | 10.019 ± 0.005 Å |
c | 15.068 ± 0.008 Å |
α | 100.372 ± 0.006° |
β | 100.796 ± 0.006° |
γ | 104.467 ± 0.006° |
Cell volume | 1198.1 ± 1.1 Å3 |
Cell temperature | 103.15 K |
Ambient diffraction temperature | 103 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.025 |
Residual factor for significantly intense reflections | 0.0236 |
Weighted residual factors for significantly intense reflections | 0.0598 |
Weighted residual factors for all reflections included in the refinement | 0.0606 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.093 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4072073.html
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Users of the data should acknowledge the original authors of the
structural data.