Crystallography Open Database

Information card for entry 4072084

4072083 << 4072084 >> 4072085

Preview

Coordinates	4072084.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52.4 H52.8 Cl0.8 N4 O10 Os4
Calculated formula	C52.4 H52.8 Cl0.8 N4 O10 Os4
Title of publication	NHC Complexes of Osmium Clusters: A Structural and Reactivity Study
Authors of publication	Cooke, Craig E.; Jennings, Michael C.; Katz, Michael J.; Pomeroy, R. K.; Clyburne, Jason A. C.
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	22
Pages of publication	5777
a	10.272 ± 0.0003 Å
b	22.8096 ± 0.0005 Å
c	24.0937 ± 0.0005 Å
α	90°
β	94.131 ± 0.001°
γ	90°
Cell volume	5630.5 ± 0.2 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0854
Residual factor for significantly intense reflections	0.0495
Weighted residual factors for significantly intense reflections	0.1192
Weighted residual factors for all reflections included in the refinement	0.1343
Goodness-of-fit parameter for all reflections included in the refinement	1.022
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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