Crystallography Open Database

Information card for entry 4072089

4072088 << 4072089 >> 4072090

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Coordinates	4072089.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H33 N2 O10 Os4
Calculated formula	C40 H33 N2 O10 Os4
Title of publication	NHC Complexes of Osmium Clusters: A Structural and Reactivity Study
Authors of publication	Cooke, Craig E.; Jennings, Michael C.; Katz, Michael J.; Pomeroy, R. K.; Clyburne, Jason A. C.
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	22
Pages of publication	5777
a	12.3074 ± 0.0004 Å
b	12.6819 ± 0.0004 Å
c	14.7598 ± 0.0005 Å
α	74.792 ± 0.002°
β	87.235 ± 0.002°
γ	62.317 ± 0.002°
Cell volume	1961.26 ± 0.12 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0552
Residual factor for significantly intense reflections	0.0513
Weighted residual factors for significantly intense reflections	0.1408
Weighted residual factors for all reflections included in the refinement	0.1448
Goodness-of-fit parameter for all reflections included in the refinement	1.04
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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