Information card for entry 4072112

Structure parameters

• Common name: {1,4-[(DIPP-NC(Me)CHC(Me)-N]2-C6H4}Ca2[N(TMS)2]2(THF)2
• Formula: C30 H52 Ca N3 O Si2
• Calculated formula: C30 H52 Ca N3 O Si2
• Title of publication: Bimetallic Calcium and Zinc Complexes with Bridged β-Diketiminate Ligands: Investigations on Epoxide/CO2Copolymerization
• Authors of publication: Piesik, Dirk F.-J.; Range, Sven; Harder, Sjoerd
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 23
• Pages of publication: 6178
• a: 34.0276 ± 0.0009 Å
• b: 10.3059 ± 0.0003 Å
• c: 19.5596 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6859.3 ± 0.3 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 6
• Space group number: 56
• Hermann-Mauguin space group symbol: P c c n
• Hall space group symbol: -P 2ab 2ac
• Residual factor for all reflections: 0.0897
• Residual factor for significantly intense reflections: 0.0495
• Weighted residual factors for significantly intense reflections: 0.122
• Weighted residual factors for all reflections included in the refinement: 0.147
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No