Information card for entry 4072152

Structure parameters

• Formula: C22.5 H51.5 I N Si2 U
• Calculated formula: C27.5 H51.5 I N Si2 U
• Title of publication: A Mild Protocol To Generate Uranium(IV) Mixed-Ligand Metallocene Complexes using Copper(I) Iodide
• Authors of publication: Graves, Christopher R.; Schelter, Eric J.; Cantat, Thibault; Scott, Brian L.; Kiplinger, Jaqueline L.
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 20
• Pages of publication: 5371
• a: 9.76 ± 0.002 Å
• b: 17.856 ± 0.004 Å
• c: 18.371 ± 0.004 Å
• α: 95.73 ± 0.03°
• β: 100.47 ± 0.03°
• γ: 93.31 ± 0.03°
• Cell volume: 3123.1 ± 1.2 ų
• Cell temperature: 141 ± 2 K
• Ambient diffraction temperature: 141 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.041
• Residual factor for significantly intense reflections: 0.0264
• Weighted residual factors for significantly intense reflections: 0.0469
• Weighted residual factors for all reflections included in the refinement: 0.0496
• Goodness-of-fit parameter for all reflections included in the refinement: 0.983
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No