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Information card for entry 4072159
Preview
Coordinates | 4072159.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C25 H33 As Cl N Pd |
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Calculated formula | C25 H31.83 As Cl N Pd |
Title of publication | Asymmetric Synthesis of a Tertiary Arsine by Nucleophilic Addition to a Chiral Phosphine-Stabilized Arsenium Salt |
Authors of publication | Coote, Michelle L.; Krenske, Elizabeth H.; Porter, Keith A.; Weir, Michelle L.; Willis, Anthony C.; Zhou, Xiangting; Wild, S. Bruce |
Journal of publication | Organometallics |
Year of publication | 2008 |
Journal volume | 27 |
Journal issue | 19 |
Pages of publication | 5099 |
a | 9.9468 ± 0.0001 Å |
b | 13.537 ± 0.0002 Å |
c | 18.6809 ± 0.0002 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2515.38 ± 0.05 Å3 |
Cell temperature | 200 K |
Ambient diffraction temperature | 200 K |
Number of distinct elements | 6 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0425 |
Residual factor for significantly intense reflections | 0.0309 |
Weighted residual factors for all reflections | 0.0362 |
Weighted residual factors for all reflections included in the refinement | 0.0321 |
Goodness-of-fit parameter for all reflections | 0.746 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.734 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4072159.html
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structural data.