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Information card for entry 4072165
Preview
Coordinates | 4072165.cif |
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Original paper (by DOI) | HTML |
Chemical name | Tetrakis-μ-(caprolactamate)-bis(acetonitrile)dirhodium(II,III) tetrafluoroborate |
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Formula | C28 H46 B F4 N6 O4 Rh2 |
Calculated formula | C28 H46 B F4 N6 O4 Rh2 |
Title of publication | Removal of Metal−Metal Bonding in a Dimetallic Paddlewheel Complex: Molecular and Electronic Structure of Bis(phenyl) Dirhodium(III) Carboxamidate Compounds |
Authors of publication | Wolf, Joffrey; Poli, Rinaldo; Xie, Jian-Hua; Nichols, Jason; Xi, Bin; Zavalij, Peter; Doyle, Michael P. |
Journal of publication | Organometallics |
Year of publication | 2008 |
Journal volume | 27 |
Journal issue | 22 |
Pages of publication | 5836 |
a | 20.7453 ± 0.0009 Å |
b | 16.8043 ± 0.0007 Å |
c | 9.9841 ± 0.0004 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 3480.6 ± 0.3 Å3 |
Cell temperature | 223 ± 2 K |
Ambient diffraction temperature | 223 ± 2 K |
Number of distinct elements | 7 |
Space group number | 62 |
Hermann-Mauguin space group symbol | P n m a |
Hall space group symbol | -P 2ac 2n |
Residual factor for all reflections | 0.0613 |
Residual factor for significantly intense reflections | 0.0331 |
Weighted residual factors for significantly intense reflections | 0.064 |
Weighted residual factors for all reflections included in the refinement | 0.0693 |
Goodness-of-fit parameter for all reflections included in the refinement | 1 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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