Information card for entry 4072267

Structure parameters

• Formula: C30 H46 Ge2 N4
• Calculated formula: C30 H46 Ge2 N4
• SMILES: [Ge]1([Ge]2[N](=C(N2C(C)(C)C)c2ccccc2)C(C)(C)C)[N](=C(N1C(C)(C)C)c1ccccc1)C(C)(C)C
• Title of publication: RGe(I)Ge(I)R Compound (R = PhC(NtBu)2) with a Ge−Ge Single Bond and a Comparison with the Gauche Conformation of Hydrazine†
• Authors of publication: Nagendran, Selvarajan; Sen, Sakya S.; Roesky, Herbert W.; Koley, Debasis; Grubmüller, Helmut; Pal, Aritra; Herbst-Irmer, Regine
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 21
• Pages of publication: 5459
• a: 20.397 ± 0.003 Å
• b: 14.12 ± 0.002 Å
• c: 21.943 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6319.7 ± 1.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0467
• Residual factor for significantly intense reflections: 0.0299
• Weighted residual factors for significantly intense reflections: 0.0661
• Weighted residual factors for all reflections included in the refinement: 0.0743
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No