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Information card for entry 4072269
Preview
Coordinates | 4072269.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C20 H33 Cl2 Ir Zr |
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Calculated formula | C20 H33 Cl2 Ir Zr |
SMILES | [IrH3]1234([Zr]5678(Cl)(Cl)[c]9([c]5([c]6([c]7([c]89C)C)C)C)C)[c]5([c]4([c]3([c]2([c]15C)C)C)C)C |
Title of publication | Synthesis and Reactivity of Early−Late Heterobimetallic Hydrides of Group 4 Metals and Iridium Supported by Mono(η5-C5Me5) Ancillary Ligands: Bimetallic Carbon−Hydrogen Bond Activation |
Authors of publication | Oishi, Masataka; Kato, Takeshi; Nakagawa, Mayuko; Suzuki, Hiroharu |
Journal of publication | Organometallics |
Year of publication | 2008 |
Journal volume | 27 |
Journal issue | 23 |
Pages of publication | 6046 |
a | 10.7052 ± 0.0003 Å |
b | 14.1183 ± 0.0005 Å |
c | 15.6994 ± 0.0006 Å |
α | 90° |
β | 105.764 ± 0.0011° |
γ | 90° |
Cell volume | 2283.55 ± 0.14 Å3 |
Cell temperature | 193 ± 2 K |
Ambient diffraction temperature | 193 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0264 |
Residual factor for significantly intense reflections | 0.0231 |
Weighted residual factors for significantly intense reflections | 0.0498 |
Weighted residual factors for all reflections included in the refinement | 0.0515 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.971 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4072269.html
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Users of the data should acknowledge the original authors of the
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