Crystallography Open Database

Information card for entry 4072284

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Coordinates	4072284.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C43 H48 Cl4 N3 P Ru
Calculated formula	C43 H48 Cl4 N3 P Ru
Title of publication	Unsymmetrical Bis(iminoethyl)pyridine Metal Complexes with a Pendant Alkenyl Substituent. Part B: Internal Olefin Coordination to Ruthenium†
Authors of publication	Wallenhorst, Carolin; Kehr, Gerald; Fröhlich, Roland; Erker, Gerhard
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	24
Pages of publication	6557
a	9.688 ± 0.001 Å
b	11.853 ± 0.001 Å
c	36.224 ± 0.001 Å
α	90°
β	93.24 ± 0.01°
γ	90°
Cell volume	4153 ± 0.6 Å³
Cell temperature	198 ± 2 K
Ambient diffraction temperature	198 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.062
Residual factor for significantly intense reflections	0.0456
Weighted residual factors for significantly intense reflections	0.1225
Weighted residual factors for all reflections included in the refinement	0.1353
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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