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Information card for entry 4072378
Preview
Coordinates | 4072378.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C28 H50 B F4 N2 P Pd |
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Calculated formula | C28 H50 B F4 N2 P Pd |
Title of publication | Design of Cationic Mixed Phosphine/N-Heterocyclic Carbene Palladium(II) π-Allyl Complexes as Monoligated Phosphine Pd(0) Precatalysts: Synthesis, Structural Studies, Catalysis, and Reactivity |
Authors of publication | Normand, Adrien T.; Stasch, Andreas; Ooi, Li-Ling; Cavell, Kingsley J. |
Journal of publication | Organometallics |
Year of publication | 2008 |
Journal volume | 27 |
Journal issue | 24 |
Pages of publication | 6507 |
a | 11.025 ± 0.002 Å |
b | 16.891 ± 0.003 Å |
c | 18.152 ± 0.004 Å |
α | 69.33 ± 0.03° |
β | 81.22 ± 0.03° |
γ | 79.61 ± 0.03° |
Cell volume | 3096.3 ± 1.2 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0706 |
Residual factor for significantly intense reflections | 0.0419 |
Weighted residual factors for significantly intense reflections | 0.0831 |
Weighted residual factors for all reflections included in the refinement | 0.0934 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.038 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4072378.html
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Users of the data should acknowledge the original authors of the
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