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Information card for entry 4072384
Preview
Coordinates | 4072384.cif |
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Original paper (by DOI) | HTML |
Formula | C24 H42.67 B0.67 F2.67 N1.33 O0.67 P0.67 Pd0.67 |
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Calculated formula | C24 H42.6667 B0.666667 F2.66667 N1.33333 O0.666667 P0.666667 Pd0.666667 |
Title of publication | Design of Cationic Mixed Phosphine/N-Heterocyclic Carbene Palladium(II) π-Allyl Complexes as Monoligated Phosphine Pd(0) Precatalysts: Synthesis, Structural Studies, Catalysis, and Reactivity |
Authors of publication | Normand, Adrien T.; Stasch, Andreas; Ooi, Li-Ling; Cavell, Kingsley J. |
Journal of publication | Organometallics |
Year of publication | 2008 |
Journal volume | 27 |
Journal issue | 24 |
Pages of publication | 6507 |
a | 10.9411 ± 0.0001 Å |
b | 19.7725 ± 0.0002 Å |
c | 17.8474 ± 0.0002 Å |
α | 90° |
β | 93.8024 ± 0.0005° |
γ | 90° |
Cell volume | 3852.48 ± 0.07 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 8 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0471 |
Residual factor for significantly intense reflections | 0.0353 |
Weighted residual factors for all reflections | 0.0913 |
Weighted residual factors for significantly intense reflections | 0.0864 |
Weighted residual factors for all reflections included in the refinement | 0.0913 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.9583 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4072384.html
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