Information card for entry 4072432

Structure parameters

• Formula: C41 H56 Br2 N4 Ni2
• Calculated formula: C41 H55.5 Br2 N4 Ni2
• Title of publication: A Nickel(II)-Cornered Molecular Rectangle with Biscarbene and 4,4′-Bipyridine Bridging Groups
• Authors of publication: Hahn, F. Ekkehardt; Radloff, Christian; Pape, Tania; Hepp, Alexander
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 24
• Pages of publication: 6408
• a: 17.3023 ± 0.0014 Å
• b: 23.345 ± 0.002 Å
• c: 23.2655 ± 0.0019 Å
• α: 90°
• β: 96.098 ± 0.001°
• γ: 90°
• Cell volume: 9344.3 ± 1.3 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1906
• Residual factor for significantly intense reflections: 0.0859
• Weighted residual factors for significantly intense reflections: 0.2493
• Weighted residual factors for all reflections included in the refinement: 0.3137
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No