Information card for entry 4072490

Structure parameters

• Formula: C23 H22 Cl N O4 Si
• Calculated formula: C23 H22 Cl N O4 Si
• Title of publication: A Disilane with a Hypercoordinate Silicon Atom: Coordination of an Imine Ligand versus Si−Si Bond Splitting
• Authors of publication: Wagler, Jörg
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 1
• Pages of publication: 155
• a: 10.1667 ± 0.0012 Å
• b: 10.609 ± 0.0012 Å
• c: 11.4683 ± 0.001 Å
• α: 116.999 ± 0.002°
• β: 92.598 ± 0.003°
• γ: 97.476 ± 0.003°
• Cell volume: 1085.1 ± 0.2 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0555
• Residual factor for significantly intense reflections: 0.0381
• Weighted residual factors for significantly intense reflections: 0.1048
• Weighted residual factors for all reflections included in the refinement: 0.1105
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No