Information card for entry 4072509

Structure parameters

• Formula: C15 H27 B4 Gd Si2
• Calculated formula: C15 H27 B4 Gd Si2
• Title of publication: Chemistry of C-Trimethylsilyl-Substituted Heterocarboranes. 33. Synthesis of Mixed-Ligand Metallacarboranes of Yttrium and Lanthanides Derived from Open η5-Pentadiene and C2B4-Carborane: A Synthetic and Structural Investigation
• Authors of publication: Wang, Jianhui; Zheng, Chong; Canseco-Melchor, Graciela; Hilby, Daniel J.; Maguire, John A.; Hosmane, Narayan S.
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 3
• Pages of publication: 577
• a: 8.388 ± 0.002 Å
• b: 11.686 ± 0.003 Å
• c: 14.244 ± 0.004 Å
• α: 72.634 ± 0.004°
• β: 73.37 ± 0.004°
• γ: 76.35 ± 0.004°
• Cell volume: 1259.4 ± 0.6 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0665
• Residual factor for significantly intense reflections: 0.0608
• Weighted residual factors for significantly intense reflections: 0.178
• Weighted residual factors for all reflections included in the refinement: 0.1823
• Goodness-of-fit parameter for all reflections included in the refinement: 1.176
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No