Information card for entry 4072639

Structure parameters

• Formula: C39 H53 Co4 O35 P8
• Calculated formula: C39 H53 Co4 O35 P8
• Title of publication: Organometallic Supramolecular Mixed-Valence Cobalt(I)/Cobalt(II) Aquo Complexes Stabilized with the Water-Soluble Phosphine Ligandp-TPPTP (p-triphenylphosphine triphosphonic acid)
• Authors of publication: Schull, Terence L.; Henley, Leila; Deschamps, Jeffrey R.; Butcher, Ray J.; Maher, Dermot P.; Klug, Christopher A.; Swider-Lyons, Karen; Dressick, Walter J.; Bujoli, Bruno; Greenwood, Andrew E.; Congiardo, Laura K. Byington; Knight, D. Andrew
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 9
• Pages of publication: 2272
• a: 31.6791 ± 0.0018 Å
• b: 22.1307 ± 0.0018 Å
• c: 29.632 ± 0.002 Å
• α: 90°
• β: 119.855 ± 0.002°
• γ: 90°
• Cell volume: 18017 ± 2 ų
• Cell temperature: 103 ± 1 K
• Ambient diffraction temperature: 103 ± 1 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0737
• Residual factor for significantly intense reflections: 0.0497
• Weighted residual factors for significantly intense reflections: 0.1309
• Weighted residual factors for all reflections included in the refinement: 0.1392
• Goodness-of-fit parameter for all reflections included in the refinement: 0.999
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No