Information card for entry 4072765

Structure parameters

• Formula: C33 H29.5 Cl0.5 N2 O5.75 Sn2
• Calculated formula: C132 H97 Cl2 N8 O23 Sn8
• Title of publication: New Structural Forms of Organostannoxane Macrocycle Networks
• Authors of publication: Chandrasekhar, Vadapalli; Thirumoorthi, Ramalingam; Azhakar, Ramachandran
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 1
• Pages of publication: 26
• a: 23.398 ± 0.005 Å
• b: 17.539 ± 0.005 Å
• c: 32.266 ± 0.005 Å
• α: 90 ± 0.005°
• β: 107.938 ± 0.005°
• γ: 90 ± 0.005°
• Cell volume: 12598 ± 5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.13
• Residual factor for significantly intense reflections: 0.0696
• Weighted residual factors for significantly intense reflections: 0.1512
• Weighted residual factors for all reflections included in the refinement: 0.1766
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No