Crystallography Open Database

Information card for entry 4072989

Preview

Coordinates	4072989.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H44 Cl3 F Ge2
Calculated formula	C38 H44 Cl3 F Ge2
Title of publication	New Digermylalkenes and Digermylalkynes: [1,3]-Chlorine Shifts in Organogermanium Chemistry?
Authors of publication	Nemes, Gabriela; Escudié, Jean; Silaghi-Dumitrescu, Ioan; Ranaivonjatovo, Henri; Silaghi-Dumitrescu, Luminita; Gornitzka, Heinz
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	21
Pages of publication	5136
a	8.4471 ± 0.0008 Å
b	28.13 ± 0.003 Å
c	15.0938 ± 0.0014 Å
α	90°
β	95.896 ± 0.002°
γ	90°
Cell volume	3567.6 ± 0.6 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0781
Residual factor for significantly intense reflections	0.0442
Weighted residual factors for significantly intense reflections	0.0845
Weighted residual factors for all reflections included in the refinement	0.0947
Goodness-of-fit parameter for all reflections included in the refinement	1.012
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4072989.html