Information card for entry 4073025

Structure parameters

• Formula: C25.75 H16 Co Fe Mo O7 P S
• Calculated formula: C25.75 H14 Co Fe Mo O7 P S
• Title of publication: Synthesis and Structural Characterization of the μ-η1:η5-Ph2PC5H4Ligand-Containing Transition-Metal Cluster and Dinuclear Complexes (μ-η1:η5-Ph2PC5H4)(μ3-S)MFeCo(CO)7(M = Mo, W), (μ-η1:η5-Ph2PC5H4)(μ3-RC)MCo2(CO)7(M = Mo, W; R = Me, Ph), and (μ-η1:η5-Ph2PC5H4)CpMo2(CO)5Obtained from the Studied Isolobal Displacement Reactions
• Authors of publication: Song, Li-Cheng; Yu, Guang-Ao; Liu, Yang; Yin, Bang-Shao; Zhang, Xiao-Guang; Hu, Qing-Mei
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 8
• Pages of publication: 1966
• a: 10.485 ± 0.006 Å
• b: 12.409 ± 0.007 Å
• c: 12.774 ± 0.007 Å
• α: 67.847 ± 0.009°
• β: 65.925 ± 0.008°
• γ: 87.486 ± 0.01°
• Cell volume: 1393.5 ± 1.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0522
• Residual factor for significantly intense reflections: 0.0352
• Weighted residual factors for significantly intense reflections: 0.086
• Weighted residual factors for all reflections included in the refinement: 0.0958
• Goodness-of-fit parameter for all reflections included in the refinement: 1.007
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No