Information card for entry 4073031

Structure parameters

• Formula: C56.5 H98 B Dy K O6
• Calculated formula: C53 H94 B Dy K O6
• SMILES: [Dy]123456789([c]%10([cH]4[c]3([cH]2[c]1%10C(C)(C)C)C(C)(C)C)C(C)(C)C)([c]1([c]5([cH]6[c]7([cH]81)C(C)(C)C)C(C)(C)C)C(C)(C)C)[H][BH2][H]9.[K]12345[O]6CC[O]5CC[O]1CC[O]2CC[O]3CC[O]4CC6.Cc1ccccc1
• Title of publication: Isolation of Stable Organodysprosium(II) Complexes by Chemical Reduction of Dysprosium(III) Precursors
• Authors of publication: Jaroschik, Florian; Nief, François; Le Goff, Xavier-Frédéric; Ricard, Louis
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 5
• Pages of publication: 1123
• a: 13.638 ± 0.001 Å
• b: 15.126 ± 0.001 Å
• c: 15.707 ± 0.001 Å
• α: 66.384 ± 0.001°
• β: 88.718 ± 0.001°
• γ: 87.166 ± 0.001°
• Cell volume: 2965.2 ± 0.3 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0481
• Residual factor for significantly intense reflections: 0.0408
• Weighted residual factors for significantly intense reflections: 0.1138
• Weighted residual factors for all reflections included in the refinement: 0.1191
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No