Information card for entry 4073204

Structure parameters

• Common name: [Y{C5Me4SiMe2(C?CCH=CHO)}(CH2SiMe3)(THF)2]
• Chemical name: [Y(C5Me4{SiMe2(C4H2O)})(CH2SiMe3)(THF)3]
• Formula: C27 H45 O3 Si2 Y
• Calculated formula: C27 H45 O3 Si2 Y
• Title of publication: Ring-Opening of a Furyl Group Appended to the Cyclopentadienyl Ligand in Rare-Earth Metal Half-Sandwich Complexes
• Authors of publication: Hitzbleck, Julia; Okuda, Jun
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 13
• Pages of publication: 3227
• a: 16.875 ± 0.004 Å
• b: 10.176 ± 0.002 Å
• c: 17.594 ± 0.004 Å
• α: 90°
• β: 99.049 ± 0.006°
• γ: 90°
• Cell volume: 2983.6 ± 1.1 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0686
• Residual factor for significantly intense reflections: 0.0408
• Weighted residual factors for significantly intense reflections: 0.0934
• Weighted residual factors for all reflections included in the refinement: 0.106
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No