Information card for entry 4073241

Structure parameters

• Formula: C34.25 H52.63 Cl N6 Si2 Y
• Calculated formula: C34 H52 Cl N6 Si2 Y
• Title of publication: Synthesis and NHC Lability of d0Lithium, Yttrium, Titanium, and Zirconium Amido Bis(N-heterocyclic carbene) Complexes
• Authors of publication: Edworthy, Ian S.; Blake, Alexander J.; Wilson, Claire; Arnold, Polly L.
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 15
• Pages of publication: 3684
• a: 15.9217 ± 0.0006 Å
• b: 31.6519 ± 0.0012 Å
• c: 18.482 ± 0.0007 Å
• α: 90°
• β: 104.618 ± 0.002°
• γ: 90°
• Cell volume: 9012.5 ± 0.6 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0578
• Residual factor for significantly intense reflections: 0.0421
• Weighted residual factors for significantly intense reflections: 0.12
• Weighted residual factors for all reflections included in the refinement: 0.1259
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.6712 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No