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Information card for entry 4073294
Preview
Coordinates | 4073294.cif |
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Original paper (by DOI) | HTML |
Formula | C71 H104 La2 O8 |
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Calculated formula | C71 H103 La2 O8 |
Title of publication | Facile Insertion of CO2into Tetra- and Pentamethylcyclopentadienyl Lanthanide Moieties To Form (C5Me4RCO2)-Carboxylate Ligands (R = H, Me) |
Authors of publication | Evans, William J.; Rego, Daniel B.; Ziller, Joseph W.; DiPasquale, Antonio G.; Rheingold, Arnold L. |
Journal of publication | Organometallics |
Year of publication | 2007 |
Journal volume | 26 |
Journal issue | 19 |
Pages of publication | 4737 |
a | 12.0519 ± 0.0015 Å |
b | 12.397 ± 0.0016 Å |
c | 12.8787 ± 0.0016 Å |
α | 68.495 ± 0.002° |
β | 74.493 ± 0.002° |
γ | 77.091 ± 0.002° |
Cell volume | 1708.1 ± 0.4 Å3 |
Cell temperature | 163 ± 2 K |
Ambient diffraction temperature | 163 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.02 |
Residual factor for significantly intense reflections | 0.0185 |
Weighted residual factors for significantly intense reflections | 0.0459 |
Weighted residual factors for all reflections included in the refinement | 0.0467 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.064 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4073294.html
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