Information card for entry 4073307

Structure parameters

• Formula: C28 H47 Lu N2 Si2
• Calculated formula: C28 H32 Lu N2 Si2
• Title of publication: Reactivity of (C5Me5)Lu(CH2SiMe3)2(THF) with Pyridine Ring Systems: Synthesis and Structural Characterization of an η2-(N,C)-Pyridyl (Mono)pentamethylcyclopentadienyl Lutetium(III) Complex
• Authors of publication: Jantunen, Kimberly C.; Scott, Brian L.; Gordon, John C.; Kiplinger, Jaqueline L.
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 10
• Pages of publication: 2777
• a: 16.225 ± 0.003 Å
• b: 11.999 ± 0.003 Å
• c: 32.866 ± 0.006 Å
• α: 90°
• β: 97.654 ± 0.004°
• γ: 90°
• Cell volume: 6341 ± 2 ų
• Cell temperature: 203 ± 1 K
• Ambient diffraction temperature: 203 ± 1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1163
• Residual factor for significantly intense reflections: 0.0688
• Weighted residual factors for significantly intense reflections: 0.1378
• Weighted residual factors for all reflections included in the refinement: 0.1498
• Goodness-of-fit parameter for all reflections included in the refinement: 1.277
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No