Information card for entry 4073364

Structure parameters

• Formula: C33 H54 B Cl F4 O Os P2
• Calculated formula: C33.019 H54 B Cl F4 O Os P2
• Title of publication: α-Substituted Alkenyl and α-Disubstituted Alkylidene Complexes with the OsCl(CO)(PiPr3)2Skeleton
• Authors of publication: Esteruelas, Miguel A.; López, Ana M.; Oñate, Enrique
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 13
• Pages of publication: 3260
• a: 10.925 ± 0.0006 Å
• b: 11.9094 ± 0.0006 Å
• c: 14.906 ± 0.0008 Å
• α: 77.707 ± 0.001°
• β: 71.233 ± 0.001°
• γ: 75.995 ± 0.001°
• Cell volume: 1762.37 ± 0.16 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0317
• Residual factor for significantly intense reflections: 0.0269
• Weighted residual factors for significantly intense reflections: 0.0564
• Weighted residual factors for all reflections included in the refinement: 0.0569
• Goodness-of-fit parameter for all reflections included in the refinement: 0.962
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No